Great example, for a novice, I just I’d like to add a few key points that were missing: 1) the sample has to be dry of solvents/water used in the recrystallisation 2) if the the sample has any crystalline properties, it needs to be ground into a uniform and homogenous amorphous solid 3) the capillaries should have between 2-5mm of sample for an accurate read 4) For a solid of known melting set tthe 20 C below expected melting point, and then for an accurate reading a temperature rise of 1 C/min is required.
Great example, for a novice, I just I’d like to add a few key points that were missing:
1) the sample has to be dry of solvents/water used in the recrystallisation
2) if the the sample has any crystalline properties, it needs to be ground into a uniform and homogenous amorphous solid
3) the capillaries should have between 2-5mm of sample for an accurate read
4) For a solid of known melting set tthe 20 C below expected melting point, and then for an accurate reading a temperature rise of 1 C/min is required.
they make these labs sound so difficult in the lab-packets. Theyre actually very easy
im so inlove with your explanation
Thank you!
thanks i learned it
coooooooooooooooooool so thanks cause i was looking for it
Whats the name of the compound?
What's the name of the substance
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Melting point lab tomorrow! Lehgo!!!!
how is it?
thank uuuuuuuuuuuuuuuuuu
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