Recrystallization and Melting Point Analysis

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  • เผยแพร่เมื่อ 4 ธ.ค. 2022
  • Now that we have covered some important separation techniques, let's take a look at a purification technique. Sometimes a chemical reaction will produce a solid, which can precipitate from solution. But these crystals typically contain impurities from solution that were trapped in the lattice as it formed. After we isolate these crystals, we can purify them via recrystallization. This is where we dissolve them in a particular hot solvent that will then retain any impurities before cooling it down such that it can crystallize again. We will also learn how to assess the purity of our recrystallized product using melting point analysis. This is neat stuff!
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ความคิดเห็น • 56

  • @nathanmermilliod3135
    @nathanmermilliod3135 ปีที่แล้ว +24

    Perfect video and explanation of concepts, and just in time for my students’ lab practical on recrystallization. Thanks Professor Dave!

    • @23100Battlefield
      @23100Battlefield ปีที่แล้ว

      I had my lab on this three weeks ago! Wish Dave had this video earlier, you really have labs late in the term, it's our exam period rn

  • @thomaseddyson362
    @thomaseddyson362 ปีที่แล้ว +7

    Thank you. I always appreciate the effort you go to with your videos. Well presented with just enough of the required ephemera.

  • @martinarenzi4744
    @martinarenzi4744 ปีที่แล้ว +2

    Thank you Prof Dave! As always so precise and clear

  • @hananehanane3860
    @hananehanane3860 ปีที่แล้ว +5

    I hope to see more techniques explanation in your channel. Thanks Prof Dave

  • @MSA_fansite
    @MSA_fansite ปีที่แล้ว +1

    I love you mr.dave you are really helping beyond imagination

  • @harrybrielmann189
    @harrybrielmann189 ปีที่แล้ว

    very complete! And I agree that trituration (forcing the solvent out by the addition of a less soluble solvent) often results in a less pure product.

  • @cancan1231ify
    @cancan1231ify ปีที่แล้ว +3

    Hey, I have friends and roommates that work for Thermo Fischer scientific. What a fun coincidence that they sponsored one of my favorite TH-camrs.

  • @louisnemzer6801
    @louisnemzer6801 ปีที่แล้ว +1

    My favorite organic chemistry purification method!

  • @prixynealojado6998
    @prixynealojado6998 6 หลายเดือนก่อน

    You're my hero, Professor Dave 🫶

  • @vspqrv9784
    @vspqrv9784 หลายเดือนก่อน

    such a high quality video and explanation

  • @nicco-sixty
    @nicco-sixty ปีที่แล้ว +6

    Will you do more in-depth concepts in multivariable calculus, like the Jacobian matrix?

  • @eddielikesfish7114
    @eddielikesfish7114 ปีที่แล้ว +4

    i literally just learnt about this in chemistry lol. we are going to be making asprin with this method in january

  • @similosihlegqalisisa8211
    @similosihlegqalisisa8211 9 หลายเดือนก่อน +1

    I'm subscribing now Prof❤❤❤

  • @ansammkh1681
    @ansammkh1681 ปีที่แล้ว

    thank you

  • @henna_nenna
    @henna_nenna 4 หลายเดือนก่อน

    you are saving the life of every ochem college student thank you so much

  • @Dylan-cv7kj
    @Dylan-cv7kj ปีที่แล้ว +27

    Science is so cool

  • @There-ought-to-be-clowns
    @There-ought-to-be-clowns ปีที่แล้ว

    Fascinating

  • @TomasElizabeth
    @TomasElizabeth 13 วันที่ผ่านมา

    So super cool

  • @milviodeleon4421
    @milviodeleon4421 ปีที่แล้ว

    Wow comments on. Good job 👍

  • @rozana4470
    @rozana4470 ปีที่แล้ว +1

    When are the other videos coming cause i start OC lab this week😭

  • @StephOnyia
    @StephOnyia 7 หลายเดือนก่อน

    You are a pro 😮 Including the guy in the laboratory 😊

  • @rassimsimou1594
    @rassimsimou1594 ปีที่แล้ว +1

    Good

  • @gamingwithrksaver4868
    @gamingwithrksaver4868 ปีที่แล้ว

    We used to do these for derivative tests... and then match the m.p. to literature value to confirm the compound

  • @missionsuccess6323
    @missionsuccess6323 8 หลายเดือนก่อน

    . Synthesis of 2-Amino-4-(substituted-phenyl)-1, 3-thi-
    azole Derivatives

  • @RevilHermes
    @RevilHermes ปีที่แล้ว +1

    I remember doing much simpler version with salt.

  • @TheCosmicGuy0111
    @TheCosmicGuy0111 ปีที่แล้ว

    Wowza

  • @WanderTheNomad
    @WanderTheNomad ปีที่แล้ว +1

    5:17 Why do we have to use the minimum amount of solvent? Is it just to avoid wasting it or something? Or is there another reason?

    • @keypo790
      @keypo790 ปีที่แล้ว

      Its because the experiments relies on Solubility Curve.

    • @user-qe8gy1zv2i
      @user-qe8gy1zv2i 9 หลายเดือนก่อน

      its better to use the smallest amount of solvent to minimize the amount of material lost by retintion in the mother liqour

  • @enzoshii
    @enzoshii 6 หลายเดือนก่อน

    Crystals did not form in our experiment. What could have gone wrong?

  • @chrisaltaawesome
    @chrisaltaawesome ปีที่แล้ว

    thank youuu

  • @krabre1848
    @krabre1848 ปีที่แล้ว +2

    hi

  • @Linda-hn3bh
    @Linda-hn3bh ปีที่แล้ว

    👍😌

  • @harrybrielmann189
    @harrybrielmann189 ปีที่แล้ว +1

    it's ok if the impurity is insoluble, just filter it out while hot.

  • @-JA-
    @-JA- ปีที่แล้ว

    🙂👍

  • @livingcodex9878
    @livingcodex9878 ปีที่แล้ว

    おはようございます

  • @judeboys6409
    @judeboys6409 ปีที่แล้ว +3

    This video reminds me of being a meth head in my 20s. Wouldn’t recommend it 😂. I used to “wash” it in acetone. To clean out impurities .. Have no clue what that was doing scientifically. But it sure made you higher 😅😮. Hey Dave. What would be the science of that lol ? You probably more an idea than I

  • @tiptop1681
    @tiptop1681 2 หลายเดือนก่อน

    Finally i can do this with my meth. Thanks

  • @worldsfinestsimp6421
    @worldsfinestsimp6421 ปีที่แล้ว

    TIGHT TIGHT TIGHT

  • @kevinxavier2986
    @kevinxavier2986 ปีที่แล้ว

    Komenke41

  • @krabre1848
    @krabre1848 ปีที่แล้ว +1

    idk whats happening but cool

    • @krabre1848
      @krabre1848 ปีที่แล้ว

      omg i remember this in year 7

  • @desmond3828
    @desmond3828 ปีที่แล้ว

    immunology?!

  • @DavidP089
    @DavidP089 ปีที่แล้ว

    2 million subs and your videos barely reach 10k views 🤔🤔🤔

  • @KasaJiso
    @KasaJiso ปีที่แล้ว

    First comment, day to of “do more flat earth vids they blew up.”
    Sorry not first I was too long to write the comment :(

    • @Gxlto
      @Gxlto ปีที่แล้ว +4

      Sorry man I dont think he will. It's kind of dead at this point. I hope he does more creationism debunking

  • @white_isnt_a_race2338
    @white_isnt_a_race2338 ปีที่แล้ว +1

    Educate me daddy