Making Methylamine 3 Ways

แชร์
ฝัง
  • เผยแพร่เมื่อ 20 ก.ย. 2024
  • In this video I demonstrate three ways of making the incredibly commonplace (but fairly tough to buy) chemical methylamine.
    I used the methylamine produced here to make a photographic developer called Metol, which I'll demonstrate in a future video.
    There are numerous other methods of making methylamine and its salts, as it is the simplest primary amine and a simple byproduct of a multitude of biological and organic decompositions, but I believe these three methods to be the most useful.
    This video was done on the behalf of several Patreon requests, and I am sorry it took so long. Hopefully it was worth the wait. Enjoy!
    Support My Channel on Patreon! / integralchemistry
    Since this is my longest video to date, I made numerous mistakes in my Narration. Many I caught during editing, but I'm sure you all will catch many more in the coming days.
    So far it's been noted that:
    At 2:22 methylene imine is being reduced and formaldehyde is oxidized. Not water.
    Note that this video involves the use of dangerous chemicals, and generates toxic gases. Nothing seen here should be reproduced except by professionals or under professional supervision. Synthesis of this chemical may violate local law or ordinance depending on your country of residence, so always check before proceeding with any chemical procedure.
    Also note that I will not now or ever be using this chemical to further manufacture any chemical that is illegal in any country, so do not ask.
    #chemistry #science #hydrogen #gas #elements #fire #chemical #industury #color

ความคิดเห็น • 330

  • @nenben8759
    @nenben8759 6 หลายเดือนก่อน +143

    I love lists!
    To-do lists, check lists, grocery lists, watch lists,
    they're all great!

  • @alch3myau
    @alch3myau 6 หลายเดือนก่อน +199

    “To my other favorite W.W. It's an honor working with you. Fondly, G.B.”

    • @Gelatinocyte2
      @Gelatinocyte2 6 หลายเดือนก่อน +17

      Willy Wonka

    • @blazeshark1
      @blazeshark1 3 หลายเดือนก่อน +4

      ​@@Gelatinocyte2 Woodrow Wilson?

    • @superman9693
      @superman9693 3 หลายเดือนก่อน +2

      Walter White?

    • @superman9693
      @superman9693 3 หลายเดือนก่อน +4

      🙌 You got me!

    • @alch3myau
      @alch3myau 3 หลายเดือนก่อน +1

      @@superman9693 No... Wonder Woman.

  • @snoowbrigade
    @snoowbrigade 6 หลายเดือนก่อน +329

    Now I just need a lung cancer diagnosis and an RV

  • @196Stefan2
    @196Stefan2 6 หลายเดือนก่อน +52

    5:50 Safety advise: I learned (during my vocational training almost 45 years ago) never-ever to set "normal" Erlenmeyer-flasks or other glassware with straight walls under vacuum due to the danger of an implosion. Only glassware with thick walls or roundbottom flasks should used for work involving vacuum. Before starting to work with vacuum, roundbottom flasks should be examined thoroughly for the absense of cracks. Btw: excellent work!

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +9

      Thank you so much! And thank you as well for the advice. I've never read about implosion under vacuum, but I have enough experience that I had a gut feeling it was a possibility. So far I've avoided it by never pulling anything near a full vacuum and compensating with higher heat. My biggest implosion concern is always the liebig condenser.. the inner wall looks very thin, but I do feel the geometry of it makes it less likely to undergo implosion.
      What do you think? Is it mostly just a concern with erlenmeyer flasks?

    • @TankR
      @TankR 5 หลายเดือนก่อน +1

      @@integral_chemistry borosilicate is a relatively brittle glass, it just has low thermal expansion so its a lot safer to use in the thermally rambunctious setting of a laboratory. Under vacuum the glass would mostly be under compression, ergo depending on the vacuum level I dont see it as being much of an issue (again depending on the depth of the vacuum. There is a reason near perfect vacuum chambers where you cant suck molecules out anymore you have to hit them with something (ie, those super freaking cool oil vapor pumps, Ben on Applied Science has a video of a fully glass one in operation. its amazing) are made out of thick metals. The atmosphere does not have a sense of humor....).
      That being said, Im not discounting the OPs experience in having glass implode under vacuum, just like with heat it can be hard to see the flaws that will make them fail. And I can absolutely see a regulator going screwy and pulling far too hard. Then all youd need is a cheap thin piece of glassware in the apparatus and its a afternoon of clean up, neutralizing, decontamination, and thinking up an excuse for the hospital burn ward (nosy bastards.....uh, or so ive been told). It sucks throwing away money like this, but take some time and test things to failure. If theyre only tested to some point, you have no idea how close that point is to the failure point. And besides, destruction makes for great (and informative) content ;)
      Be safe, mate! I want to see more awesome videos!

  • @DangerousLab
    @DangerousLab 6 หลายเดือนก่อน +80

    Edgy synthesis presented educationally!👍

    • @DangerousLab
      @DangerousLab 6 หลายเดือนก่อน +5

      Btw the thermometer-stirring is brutal!

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +24

      Yeah I've been good about not doing it for several months now so watching it back in editing physically hurt me. Not looking forward to how many times I'm gonna get called out on that 😅
      But thank you! "Edgy synth presented educationally" is exactly what I was going for. I think it is a really cool process from a scientific perspective, and so I wanted to show it without risking any flak from TH-cam. I think it's delivery is so void of any drug glorification and dry enough that it should hold up.
      As a side note I've been sitting on synthesis vids for TNT, RDX, and acetone peroxide for ages for the same reason I sat on this video for ages.

    • @DangerousLab
      @DangerousLab 6 หลายเดือนก่อน +1

      @@integral_chemistry Don't worry about the thermometer-stirring, we have all been there.
      Those energetic material syntheses are as edgy if not more, it would be risky to be taken down somehow but that totally depends on the YT reviewer's decision (Which is rather inconsistent), I do think those rules are less strict than before as I can see some of those edgy videos resurfaced.

    • @andrewbounds
      @andrewbounds 6 หลายเดือนก่อน +6

      ​I would avoid the acteone peroxide. I never made it and still had the ATF on me about it.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      @andrewbounds yeah thats the feeling I got.. I scrapped it and I guess I'll go ahead and toss the footage too 😅

  • @aqua-op
    @aqua-op 6 หลายเดือนก่อน +477

    Love increasing my inclusion on intelligence agency lists!

    • @markbledsoe1664
      @markbledsoe1664 6 หลายเดือนก่อน +13

      Same. I have another good channel if you want one

    • @R-C-R
      @R-C-R 6 หลายเดือนก่อน

      @@markbledsoe1664 what the the name

    • @ioioire4684
      @ioioire4684 6 หลายเดือนก่อน

      iiiiii doooooo@@markbledsoe1664

    • @albedo6300
      @albedo6300 6 หลายเดือนก่อน

      @@markbledsoe1664 I want plz

    • @jamesneufeld6308
      @jamesneufeld6308 6 หลายเดือนก่อน

      ​@markbledsoe1664 yes please

  • @kenbrady119
    @kenbrady119 6 หลายเดือนก่อน +10

    I've always admired the historic chemists like Lavoisier and Davy and so many more. Like theirs, this chemistry explores new territory. You seem to already know far more about methylamine hydrochloride than does Wikipedia does about methylammonium chloride. Thank you for letting us observe your process so clearly.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +3

      Thank you so very much, it means a lot. I do try and be creative and informative in all my work, and I'm so happy it doesn't go unnoticed.

  • @victoryfirst2878
    @victoryfirst2878 6 หลายเดือนก่อน +15

    I just love the way you did the experiment Sir. The government watch list stuff is such a double edged sword. They tell you one thing and enforce the other. A double standard to say the least .

    • @Sniperboy5551
      @Sniperboy5551 6 หลายเดือนก่อน +4

      I mean, a “watch list” just means they watch it. Those chemicals aren’t illegal to possess, synthesize or distribute. Just don’t have any Sudafed in your medicine cabinet…

    • @victoryfirst2878
      @victoryfirst2878 6 หลายเดือนก่อน +1

      THAT IS A FACT FELLA. @@Sniperboy5551

    • @UrbanPovertist
      @UrbanPovertist 6 หลายเดือนก่อน

      ​@@Sniperboy5551actually the process makes no need for Sudafed. LoL but more money can be made selling purified chemicals than gold and oil combined

    • @UrbanPovertist
      @UrbanPovertist 6 หลายเดือนก่อน +2

      Just don't store intermediates, who knows what those watchlists test for. A innocent intermediate can get you in trouble. Always go through the process or at least have your work up papers handy for intentions

    • @ARockRaider
      @ARockRaider 5 หลายเดือนก่อน +1

      the government would hardly let you have water if they could get away with it.

  • @andrews.4780
    @andrews.4780 6 หลายเดือนก่อน +25

    I love when my favorite TH-cam chemists make watchlist chemicals lol. The synthesis be looking so interesting but I won’t risk attempts at it myself because here in the states certain restricted chemicals are taken very seriously when manufactured or possessed. That’s what you guys are here for! ☺️👌🏼

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +7

      I agree with that, this isn't something I'd ever do if I didn't have this whole channel to legitimize its synthesis. If I was just doing this as a small-scale hobby I'd never want this just lying around.. even though it's legal, the optics are bad.

    • @Sniperboy5551
      @Sniperboy5551 6 หลายเดือนก่อน +4

      TH-cam has recommended a video on P2P purification to me… I just like watching chemistry

    • @andrews.4780
      @andrews.4780 6 หลายเดือนก่อน +1

      @@Sniperboy5551 that part! I’ve seen a few. I’ve literally seen the synthesis of methamphetamine base by the Lukehart reduction by a channel called TDC and it randomly popped up in my feed because of watching chemistry videos. 🤔🧐

    • @黄蟮
      @黄蟮 6 หลายเดือนก่อน

      ​@@integral_chemistryBro, have you ever made oxytocin? I'm very curious about this. How is it extracted from the ergot fungus? I really want to extract it myself. Can you teach me?

    • @bval2201
      @bval2201 หลายเดือนก่อน +1

      I think you can legally manufacture list chemicals for use in on going synthesis as long as you don't sell them

  • @doomtho42
    @doomtho42 5 หลายเดือนก่อน +2

    I just discovered this channel, but I regularly watch multiple other chemistry channels and I have to say that this one really stands out (from what I’ve seen so far) in terms of the pacing and level of detail/explanation. While I certainly enjoy the other chemistry channels I follow (I mean, obviously, because why else would I continue watching them?), each of them is just slightly off from what would be ideal for me in one or both of those aforementioned aspects - a bit too high-level, a tad more assumed knowledge than I possess, a beat slower or faster paced than my attention span and mental processing are equipped to handle, you get the idea. But this channel has been almost perfectly in-tune with my preferences on all counts. I’ve been able to follow along in real-time (i.e. without the need to frequently pause/rewind, or else fail to retain certain details) with full comprehension, and at the same time there has been very little of the unnecessary or redundant information (again, for my level of knowledge and comprehension) that typically causes my mind to wander.
    tl;dr - Cool channel bro.

  • @s0kulite
    @s0kulite 5 หลายเดือนก่อน +5

    Excellent production, Bravo Vince!

  • @R-C-R
    @R-C-R 6 หลายเดือนก่อน +84

    Next Methamphetamine

    • @chemistryofquestionablequa6252
      @chemistryofquestionablequa6252 6 หลายเดือนก่อน +49

      I mean, it’s only like 2 extra steps depending on the starting materials.

    • @R-C-R
      @R-C-R 6 หลายเดือนก่อน

      @@chemistryofquestionablequa6252 Phenylacetone and Methylamine

    • @lrrrruleroftheplanetomicro6881
      @lrrrruleroftheplanetomicro6881 6 หลายเดือนก่อน +11

      Nope, let's make mescaline instead.

    • @chemistryofquestionablequa6252
      @chemistryofquestionablequa6252 5 หลายเดือนก่อน

      @@jocm99 just look it up, TH-cam will delete it if I write it.

    • @frossbog
      @frossbog 5 หลายเดือนก่อน +1

      P2P cook. And it it ain't blue, it ain't right.

  • @midwestchem368
    @midwestchem368 6 หลายเดือนก่อน +6

    This was very detailed and informative great video man! My favorite method for this is methanol and sulfamic acid. Very cheap and very easy!

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      I was considering that one, still might do it at some point.
      But thank you so much! This video took ages so I'm glad it's appreciated

  • @johndeaux8815
    @johndeaux8815 6 หลายเดือนก่อน +30

    I'm not living in America, but I'll have fun watching this with my personal CIA agent at Pine Gap here in Australia 😂

    • @TankR
      @TankR 5 หลายเดือนก่อน +2

      If you ever want to pissed them off download the 10hr he-man hey yeah video, reencode it (so the file hash changes), name it something interesting like maybe a color with a type of dwelling followed by the thing we walk on and another word for an idea or Body Oder Mother Board (get it?), and reupload it. Some poor sod will have to sit through all 10hrs to make sure its clean ;)

    • @ahmaudarberywasaviolentkle8094
      @ahmaudarberywasaviolentkle8094 5 หลายเดือนก่อน +1

      ​@@TankR ?

    • @TankR
      @TankR 5 หลายเดือนก่อน +2

      @@ahmaudarberywasaviolentkle8094 What part are you confused on? The get a long video, ie he-man hey yeah, part, the name it something potentially of national security interest part, or the thus force an agent to watch 10 hours of hey yeah part because the video is just the original but reencoded so it wont match the hash of a known file part?

    • @ahmaudarberywasaviolentkle8094
      @ahmaudarberywasaviolentkle8094 5 หลายเดือนก่อน +2

      @@TankR too cryptic.

    • @TankR
      @TankR 5 หลายเดือนก่อน

      @@ahmaudarberywasaviolentkle8094 get some crayons and some paper, work through it. Youll get it, champ ;)

  • @AnnFranksUrn
    @AnnFranksUrn 5 หลายเดือนก่อน +17

    Proud to be joining the watchlist with you all

    • @ChiefWombatCuddler
      @ChiefWombatCuddler 4 หลายเดือนก่อน +2

      Been on it for decades now 😂😂

  • @yorkshirechemist
    @yorkshirechemist 6 หลายเดือนก่อน +1

    these are all good reliable procedures, but my personal favourite, and one of the most efficient with least waste, is one I've not yet seen demonstrated on TH-cam
    it's the reduction of formaldoxime to methylamine; formaldoxime can be formed from the reaction between formaldehyde and hydroxylamine in basic conditions

  • @s.sradon9782
    @s.sradon9782 5 หลายเดือนก่อน +5

    I want to see a future where amateur chemists just synthesize everything from air and seawater.

  • @JimmyJohnson-uq6um
    @JimmyJohnson-uq6um 4 หลายเดือนก่อน +1

    God Bless You!
    It is close to being the fountain of youth. One that should always be with our people in peace and in battle.

  • @jirischimer9540
    @jirischimer9540 6 หลายเดือนก่อน +5

    Excellent video, would love to see the reaaction with bromine

  • @-r-495
    @-r-495 6 หลายเดือนก่อน +1

    Beautiful crystals, I will out myself as someone who enjoys watching it.
    Well paced video too, sometimes I think stuff is often rushed when one shall rush on ones own peril only.

  • @ShepherdsChapelonYT
    @ShepherdsChapelonYT 4 หลายเดือนก่อน +1

    I got clean and off the streets in 94 after I got out of jail I went to work rehabilitation and here's the best thing I ever found since Shepherd's Chapel on YT explains the whole Bible God bless

    • @pnz3
      @pnz3 3 หลายเดือนก่อน

      how long were u in jail

  • @ShaneMclane-PrivateEye
    @ShaneMclane-PrivateEye 5 หลายเดือนก่อน +13

    My uncle used to make something like this in the trailer on the side of the house. He's in prison, but it seemed like he had a good time getting there. He really loves chemistry.

  • @Glitchbound
    @Glitchbound 5 หลายเดือนก่อน +2

    😂 great video! I’m never going to use this knowledge, but I love collecting dangerous information. This channel is perfect for that! I’m gonna watch your making TNT video next 👍. The commentary is good too! You are very easy to understand and explain it in a way where I know what’s happening at least. I only have taken like 3 chem classes in college and I can still get the gist of it. Subbed for sure! 👌

    • @integral_chemistry
      @integral_chemistry  5 หลายเดือนก่อน +2

      Thank you so much! These are my favorite type of comments, and I deeply appreciate hearing that some people get the things out of my work that I intended. Very happy to have you along :)

    • @Glitchbound
      @Glitchbound 5 หลายเดือนก่อน

      @@integral_chemistry No problem, thank you for the content! Have a great day 👍

  • @chemistryofquestionablequa6252
    @chemistryofquestionablequa6252 6 หลายเดือนก่อน +21

    I will certainly not use this knowledge for evil…

  • @searsbear7965
    @searsbear7965 5 หลายเดือนก่อน

    Man I love feeling wanted and this is exactly what I needed for that

  • @haebouscorpus1450
    @haebouscorpus1450 5 หลายเดือนก่อน

    Thank you for being very informative and giv8ng a great step by step on your chemistry.

  • @Kittensett
    @Kittensett หลายเดือนก่อน +2

    It's an honour getting in the watchlist with you all

  • @hattree
    @hattree 6 หลายเดือนก่อน +3

    I saw something about a family member find. When my parents passed, they had a big brown glass jug of Chlordane. It took us quite a while to find someone who would take it.

    • @daveeyes
      @daveeyes 3 หลายเดือนก่อน

      Chlordane!!! Been a long time since I gave seen that name!

  • @explorecriminalminds
    @explorecriminalminds 4 หลายเดือนก่อน +1

    I'm intrigued brother. Good content education is key

  • @Antron_Edition
    @Antron_Edition 5 หลายเดือนก่อน +6

    Programmed cell death guy tells us alternatives to raiding a warehouse with thermite.

  • @mel_with_b
    @mel_with_b 16 วันที่ผ่านมา

    Hexamine to methylamine
    Have you tried using less water to start out with? I use about fivehundred milliliters for 80 g of hexamine.
    When you add the hydrochloric acid, make sure the reaction doesn’t reach a temperature over 50°C . I use an ice bath at the beginning when I add the hydrochloric acid. And also give it about 3 to 4 hours of stirring, instead of the 2 to 3.
    And when you heat it up, i keep the temperature around 90°C.

  • @lydierayn
    @lydierayn หลายเดือนก่อน +2

    "I do not know how to make methylamine. I usually just use the barrel with the bee on it"

  • @J3553l
    @J3553l 19 วันที่ผ่านมา

    I taking this to straight to Heisenburg!!!!

  • @carrionstorm736
    @carrionstorm736 5 หลายเดือนก่อน

    This is really interesting. I'm glad you did it so I don't have to, you brave soul 😂 I would absolutely love to see how it turns out using bromine though

  • @TeresaArthur-mq3dv
    @TeresaArthur-mq3dv 5 หลายเดือนก่อน +1

    Bad things are not the worst things that can happen to us. Nothing is the worst thing that can happen to us!

  • @roqua
    @roqua 2 หลายเดือนก่อน +4

    The patrons remembered that Jesse Pinkman was flown to Mexico to instruct in the P2P method, asks for methylamine to get started and is told by the up-staged head chemist that they synthesize their own and don't carry stock on hand. Which of these three methods should a high school chemistry flunky select when attempting to fool said chemist into believing he actually knows his chemistry? My guess, one of the first two methods... you seem to know what you are doing and the hexane rearranging threw you a little curve ball. 😆

  • @victorprokop9343
    @victorprokop9343 6 หลายเดือนก่อน +4

    now i have a trusty base for a henry reaction!! Thanks brother
    what is there a black cadillac on my door

  • @eastindiaV
    @eastindiaV หลายเดือนก่อน

    It's a gas. You can use rhizobia bacteria to produce nitrogen gasses like ammonia and n20,
    Which, when bubbled through methanol using simple pressure from fermentation, (methanol is produced by anaerobic fermentation of sugars by yeast)
    Produces methylamine gas, which bubbles again, into a compressor, and into a K-Tank.

  • @chemicalmaster3267
    @chemicalmaster3267 6 หลายเดือนก่อน +4

    @Apoptosis Just if you don´t know there is a name for that extreme hygroscopicity of methylamine hydrochloride: deliquescence. It´s when a compound absorves so much moisture that it dissolves and turns into a puddle of concentrated solution.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      I've read that before, unfortunately it's one of those words I've only ever read and never heard someone say out loud so I've been holding off on the embarrassment of the whole internet hearing me mispronounce it 😬

    • @chemicalmaster3267
      @chemicalmaster3267 6 หลายเดือนก่อน +1

      @@integral_chemistry Well, I don´t blame or judge you if you have mispronounced it! I know it´s nothing serious.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      @chemicalmaster3267 lol well thank you! I'll do my best to give it a shot next time it comes up, although to save my sanity I usually avoid working with deliquescent chemicals. They're the worst

    • @chemicalmaster3267
      @chemicalmaster3267 6 หลายเดือนก่อน

      @@integral_chemistry Yeah, it´s almost impossible to do good weight measurements with them. They really are infuriating!

  • @MaksBrochu
    @MaksBrochu 4 หลายเดือนก่อน

    Hello personal RCMP/NSA agent ! Hope you enjoyed the video too

    • @JimmyJohnson-uq6um
      @JimmyJohnson-uq6um 4 หลายเดือนก่อน

      RCMP what a joke.
      Canaduh is junkies holes

  • @SyukurAzmiHoHan
    @SyukurAzmiHoHan หลายเดือนก่อน +1

    Terima kasih!

  • @williambouthillier8611
    @williambouthillier8611 6 หลายเดือนก่อน +1

    Nice video! For the Hoffmann rearrangement, the methyl group is one of the worst migrating group in such reactions so I'm not surprised you're having a hard time with it. Bromine oxidation might be faster which could avoid competing side-reactions, but other than that I don't see how you could improve the migration of the methyl group just by using another oxidizer

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      Huh yeah I hadn't even considered that angle. My thinking was perhaps a calcium-methylamine complex or double-salt formation. I do agree though, at least in my own experience for this channel I've done a Hofmann rearrangement in making hydrazine and anthranilic acid, and they both worked very well and wete FAR less temperature sensitive.
      The wild part is this exact synthesis was the very first Hofmann rearrangement, and the one the entire mechanism was based on (although I might need to fact check that)

  • @balibo07
    @balibo07 5 หลายเดือนก่อน +10

    Jesse we need to cook

    • @andresalvarez7664
      @andresalvarez7664 5 หลายเดือนก่อน

      😅 Just that Jesse needs...

    • @redbigapplefloppa302
      @redbigapplefloppa302 4 หลายเดือนก่อน +1

      Jassy.... wheres the cocainer??!

    • @MrMartinswan
      @MrMartinswan 2 หลายเดือนก่อน

      Hay anyone know away round (lah)?

    • @Flesh_Wizard
      @Flesh_Wizard 21 วันที่ผ่านมา

      Jesse we need 20003 km/h of methé

  • @whyrwehere
    @whyrwehere 3 หลายเดือนก่อน +2

    I robbed a train for this stuff and you're telling me I can just make it myself?

  • @jozefnovak7750
    @jozefnovak7750 6 หลายเดือนก่อน +1

    Super! Thank you very much!

  • @sujay_691_
    @sujay_691_ 2 หลายเดือนก่อน +1

    Still better than robbing a train.

  • @JohnLeePettimoreIII
    @JohnLeePettimoreIII 6 หลายเดือนก่อน +2

    0:11 it's also a rocket fuel, a dessert topping, a feminine hygiene spray, and a bumper polish.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      It's so widely used it is frankly bizarre it is regulated the way it is.

  • @ShadowIsHigh
    @ShadowIsHigh หลายเดือนก่อน

    Hell yeah, now I don't have to hijack a train to steal it

  • @jamiemoore1056
    @jamiemoore1056 3 หลายเดือนก่อน

    Could you please show diethylamine and triethylamine also, for the the learnings. I can't afford college and I'm starting to get basics in all areas, reasoned with old world beliefs

  • @A1ko_
    @A1ko_ 6 หลายเดือนก่อน +4

    Now as a part 2 do nitroethane, trust me it's very funny

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      LMAO I don't know about all that

    • @A1ko_
      @A1ko_ 6 หลายเดือนก่อน

      @@integral_chemistry just go to Russia or some shithole ez

    • @Gelatinocyte2
      @Gelatinocyte2 6 หลายเดือนก่อน

      Is nitrous oxide involved, somehow?

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      @Gelatinocyte2 no, but I can't really explain without getting in trouble so just Google it (because somehow Wikipedia can get away with detailed instructions for making literally anything)

    • @A1ko_
      @A1ko_ 6 หลายเดือนก่อน

      @@Gelatinocyte2 no but trust me nitroethane is how you actually end up on a government watchlist

  • @markusritter9891
    @markusritter9891 3 หลายเดือนก่อน

    an explicit instruction on how to produce raw materials for XTC and methamphetamine?!
    The police should be interested in this no matter where they are😮

  • @NapoleonGelignite
    @NapoleonGelignite 6 หลายเดือนก่อน +1

    Separating MeNH2.HCl and NH4Cl is best achieved using chloroform - methylamine salts are soluble in CHCl3

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      DCM as well yeah? I'd have definitely gone that route if only those were easier for me to buy *sigh*

  • @myristicinman4566
    @myristicinman4566 6 หลายเดือนก่อน +3

    Awesome. Are you familiar with the sulfamic acid/methanol method?

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +5

      Thank you! And yes I was actually considering adding that as a 4th method, but the length of the video would just have gotten far beyond what I'd wanna edit. I may do a part 2 with that method, paraformaldehyde, and possibly glycine decomposition because on paper that should work

    • @myristicinman4566
      @myristicinman4566 6 หลายเดือนก่อน +1

      @@integral_chemistry Please do! Love ur stuff m8, keep it up!

  • @JoshWallace-i3l
    @JoshWallace-i3l 5 หลายเดือนก่อน

    That train theft in breaking bad was about $300 million. Biggest heist ever

  • @FBI_Master
    @FBI_Master 6 หลายเดือนก่อน +1

    Walter, You have the right to remain silent.

  • @markdennison6345
    @markdennison6345 6 หลายเดือนก่อน

    Did you use boiling chips or pumice in your distillations? I assume you did. Important info for newbies! Always use a boiling chip if you're not using a stir bar. It could make you or break you!!! Literally!
    Also formaldehyde exists as formalin, usually 37%.
    (Upon further viewing I see a stir bar in there)

  • @Sniperboy5551
    @Sniperboy5551 6 หลายเดือนก่อน +3

    I got an ad for “NYC Muslim Center” entirely in Arabic when I clicked on this video… 😂 wtf

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      That is really weird.. maybe only a handful of companies want to put their ads on this 🥺

    • @Sniperboy5551
      @Sniperboy5551 6 หลายเดือนก่อน

      @integral_chemistry Cool video though, my friend. I’m not a chemist, but I enjoy watching chemistry. Great editing as well!

  • @tradward
    @tradward 6 หลายเดือนก่อน +1

    Your honour, I'm simply a victim of the youtube algorithm and nothing more.

  • @metrologic5000
    @metrologic5000 6 หลายเดือนก่อน +4

    Well tell me I can't have something and what is the first thing I'm going to want.

  • @justinblaise4176
    @justinblaise4176 6 หลายเดือนก่อน +2

    At 16 min, do you mean suck back or is the dissolution of methylamine so exothermic that the collection beaker contents heating to reflux is a concern?

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      I meant suck-back. Idk why but I've always called that reflux along with actual reflux (the kind you do intentionally with a condenser).
      But yeah it'll suck-back HARD. Much worse than ammonia or HCl

  • @UnkoHoloHolo
    @UnkoHoloHolo 4 หลายเดือนก่อน

    Feather crystals. Mahalo
    Well put across. 🤙

  • @ffggvfg4323
    @ffggvfg4323 5 หลายเดือนก่อน

    Dame bro this interaction bout to be lit

  • @robertkeyes258
    @robertkeyes258 6 หลายเดือนก่อน +1

    I recall reading somewhere a long time ago that simple thermal degradation of hexamine produces methylamine.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      It does! It's in a gaseous form though so a bit tough to collect, but yeah hexamine does slowly decompose to methylamine even at room temp.. which is why hexamine smells like rotten fish sometimes

    • @robertkeyes258
      @robertkeyes258 6 หลายเดือนก่อน

      @@integral_chemistry so you're saying if you put hexamine on a hot plate, do it in a hotel room? ;)

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      @robertkeyes258 LMAO that would be quite a mean prank 🤣 stuff smells absolutely foul and really sticks around

    • @robertkeyes258
      @robertkeyes258 6 หลายเดือนก่อน +1

      @@integral_chemistry Indeed it would. That's not something I would do.

  • @praetorian8735
    @praetorian8735 6 หลายเดือนก่อน +3

    Try the vacuum reflux method!!

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      I think I definitely will! I also wanna try paraformaldehyde instead of formalin bc that should work the same

    • @黄蟮
      @黄蟮 6 หลายเดือนก่อน

      ​@@integral_chemistryBro, have you ever made oxytocin? I'm very curious about this. How is it extracted from the ergot fungus? I really want to extract it myself. Can you teach me?

    • @黄蟮
      @黄蟮 6 หลายเดือนก่อน

      ​@@integral_chemistryOxytocin, the love hormone, is very mysterious. I searched in more than a dozen languages ​​just to find out how to prepare it and how to prepare it, but I couldn’t find how to prepare it. If you make a video, the number of views will definitely exceed 100 million. , because I feel that not only I want to watch it, but fans all over the world want to watch it.

  • @jastintheceooffinanasapost6204
    @jastintheceooffinanasapost6204 5 หลายเดือนก่อน

    I'm so sure i'm on a list now

  • @erlejomo
    @erlejomo 3 หลายเดือนก่อน +1

    the video jesse pinkman needs

  • @iancarlson-w8m
    @iancarlson-w8m 4 หลายเดือนก่อน

    Beats huffing wood polish any day!

  • @kinexkid
    @kinexkid 6 หลายเดือนก่อน +1

    I found a random bucket that's disintegrating in my grandma's back yard. The top was broken and it was flooded with rain water, but it was filled with small yellow pellets that werent dissolving, which I believe to be sulfur pastille. I'm going to "help" her dispose of it because it's like 10 pounds at least. How would I go about confirming it is sulfur and not some other random fertilizer my grandpa bought and subsequently left us when he died?

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      Very cool find! I'd say easiest way is probably to try burning it with a lighter. If it starts burning with a cool blue flame, melts into a black goo, and smells sulfurous than it's definitely sulfur.
      You could also just break a pellet open and smell, sulfur has a really distinct smell to it that's tough to get off your hands.
      Oh and it's insoluble in literally everything except toluene

    • @kinexkid
      @kinexkid 6 หลายเดือนก่อน

      I'll for sure be going back within a week to get it! Jokes aside, I do want to get it off her property. She's 86 years old and had no idea it was there. The 5 gallon bucket it was being held in is being held together with a hope and a prayer. It was so sun bleached that the bucket was breaking if you looked at it funny. I'm going to try growing some rhombic sulfur crystals with it

  • @daveanderson718
    @daveanderson718 5 หลายเดือนก่อน

    thank you!!

  • @godlugner5327
    @godlugner5327 5 หลายเดือนก่อน +1

    "it's in the barrel with the bee on it"

  • @oxylepy2
    @oxylepy2 4 หลายเดือนก่อน

    Oh no my cell membrane!!!
    Ruptures

  • @popescucristian8978
    @popescucristian8978 6 หลายเดือนก่อน +1

    this explains why your name shows up 3 times on the fbi list with the same date

  • @experimental_chemistry
    @experimental_chemistry 6 หลายเดือนก่อน +1

    Did you work under a fumehood?
    I have absolutely no use for MA, so I never synthesized it yet.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      I did 100% of synthesis #3 and portions of the first two under a fume hood, instead just feeding the gas outlet outside. Honestly should have all been done under a fume hood given the reactions going on are fairly complex and I'm not 100% certain on all potential byproducts.
      And yeah.. I only made it to make the photographic developer Metol, which is insanely overpriced so I thought this would pair well with my hobby photography. I'm having a tough time synthesizing the other requisite chemical (hydroquinone) in a pure enough state to actually use. TBH trimethylamine is much more useful than methylamine in the kind of projects I'm working on.

    • @experimental_chemistry
      @experimental_chemistry 6 หลายเดือนก่อน

      Ah yes, metol is really useful but indeed expensive.
      I am curios about the synthesis if you will show it.
      Hydroquinone is cheap and easy to get where I live but also a potential carcinogen.

  • @crazystupidgamer
    @crazystupidgamer 6 หลายเดือนก่อน +1

    Just do go chucking pizzas on your roof. Its highly suspicious.

  • @ЯрославТаран-ъ6л
    @ЯрославТаран-ъ6л หลายเดือนก่อน +1

    can i use sodium hypochlorite instead of calcium?

    • @integral_chemistry
      @integral_chemistry  หลายเดือนก่อน

      Yep, and in retrospect I actually think sodium hypochlorite would work better. Calcium hypochlorite is pretty bad at Hoffman reactions I've found.

  • @user-cb3qr9dt2k
    @user-cb3qr9dt2k 6 หลายเดือนก่อน +1

    Any Chemist can make any chemical from anything, I don't care how many you ban.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      Yeah the whole notion of banning chemicals is absurd

  • @kevinmarrs3372
    @kevinmarrs3372 6 หลายเดือนก่อน +2

    Correction at 2:22
    Methyleneamine gets reduced to methylamine
    Formaldehyde gets oxidized to Formic acid
    (The water is not being oxidized)

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +2

      Ah yeah thanks for the catch, I'll edit that into the vid description or something.
      I managed to misspeak a weird number of times in this vid (still working on my confidence on mic).
      Managed to catch most of my mess-ups but that one slipped by 😅

  • @ashvio
    @ashvio 5 หลายเดือนก่อน

    my curiosity outweighed my desire to remain off government lists

  • @Sonex1542
    @Sonex1542 6 หลายเดือนก่อน +4

    I consider myself a post cursor.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      LMAO I had to read this literally 10 different times before the pun clicked

  • @ricktroxell6448
    @ricktroxell6448 3 หลายเดือนก่อน

    What exactly is this I understand it's a precursor but to what extent

  • @GuidoChiabrera
    @GuidoChiabrera 5 หลายเดือนก่อน +2

    So why did Walter do not make his own and went under all the chaos?

    • @integral_chemistry
      @integral_chemistry  5 หลายเดือนก่อน +3

      Probably just to add a plot point. That show has quite a few silly plot points like that. I imagine Walt didn't want to make methylamine himself because it would have added a long extra step to a process he already barely had time for 😅

    • @avo616
      @avo616 4 หลายเดือนก่อน

      Why make when can steal

  • @peterinbrat
    @peterinbrat 5 หลายเดือนก่อน +1

    Still waiting on the coffee making video pulling a slight vacuum to keep the boiling point at 92°C.

    • @integral_chemistry
      @integral_chemistry  5 หลายเดือนก่อน

      Ohhh yeah I seem to vaguely remember that request actually (its been a while). I've been meaning to do more extraction type stuff anyway so maybe I'll finally give that a shot.

    • @peterinbrat
      @peterinbrat 5 หลายเดือนก่อน

      @@integral_chemistry It would be interesting to see if you could measure several components of what makes a cup of coffee good or bitter. I use a Moka Pot to brew.

  • @DJ-fn3jm
    @DJ-fn3jm 4 หลายเดือนก่อน

    That could have been an interesting story line in BB. make the Methylamine instead of stealing it.

  • @alish5417
    @alish5417 หลายเดือนก่อน

    In propellents no .
    Make it from methanol ,make a catalyst first ,and u dont have to stay near the reactor ,keep the mask away ,wear it when you want to check the prlgress ,wear a war grade mask

  • @djchlebku2603
    @djchlebku2603 6 หลายเดือนก่อน

    Amines complex with calcium ions, so yeld would be lower if you use calcium hypochloride

  • @user-qj8is8wi1p
    @user-qj8is8wi1p 6 หลายเดือนก่อน

    good night. from Colombia. How is perchloric acid made? and hydrogen peroxide

  • @RudiRidam
    @RudiRidam 4 หลายเดือนก่อน

    Hello, I'm Rudi from Indonesia, can you tell me the ingredients used in cooking meth

  • @user-cb3qr9dt2k
    @user-cb3qr9dt2k 6 หลายเดือนก่อน +1

    Nice Video

  • @jamiemoore1056
    @jamiemoore1056 3 หลายเดือนก่อน

    Can you not use trimethylamine to make vapour methylamine

  • @seditt5146
    @seditt5146 6 หลายเดือนก่อน

    There is an extremely simple method that has been skipped and is not well know which also has a benefit of being able to produce nitroethane is MeOH is replaced by EtOH and the rearrangement done in the presence of Sodium nitrite. You boil, Sulfamic acid( I believe that is what it is its been like a decades since I study chemistry, its used to clean coffee makers and tons of other stuff dirt cheep) in methyl alcohol. Reflux this until its all consumed then ramp up the temperature and you are left with methylamine after a rearrangement. You cant use it for Ethylamine unfortunately because the high temperature rearrangement does not go as planned with higher alcohols but they are powerful ethylating agents before the rearrangement meaning Sodium Nitrites will yield Nitroethane. I gotta get back to you on the Cleaning agents name, its like, sulfonic acid amide or some shit like that. I did a write up on Science madness some years ago on the process. Only down side is you need to keep water out but that was not hard at all and I did it in a kitchen chemistry setting. High yields, large possibilities and dirt dirt cheep, my opinion it is the best method around.
    [edit: Its Sulfamic Acid. You boil that in dry MeOH until the crystals are consumed, then jack up the temperature at which point you are left with Methylamine Sulfate. ]

  • @NiC.kChenNC
    @NiC.kChenNC 6 หลายเดือนก่อน +1

    This is crazy

  • @JohnLeePettimoreIII
    @JohnLeePettimoreIII 6 หลายเดือนก่อน +2

    formic acid = ant squeezins

  • @BVIAS
    @BVIAS 4 หลายเดือนก่อน

    R.I.P. Drew Sharp 🕷️

  • @nunyabisnass1141
    @nunyabisnass1141 6 หลายเดือนก่อน +2

    I use precursors to clean my damned boat and disinfect wounds for crying outloud. Also, 20% hydrogen peroxide will make the self checkout go all disco ball and shut down until an employee can confiscate it. They occasionally stock it accjdentally.

    • @chemistryofquestionablequa6252
      @chemistryofquestionablequa6252 6 หลายเดือนก่อน +3

      The real skill is being able to buy all your precursors in one purchase without anyone knowing what’s possible with them.

    • @nunyabisnass1141
      @nunyabisnass1141 6 หลายเดือนก่อน +1

      @@chemistryofquestionablequa6252 im paranoid. I feel like in the back of my mind certain products purchased together or in certain quantities triggers an alert to some agency.

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน

      I'm hoping that between this channel and the vast scope of completely unrelated chemicals I own at this point that if anyone ever decided I needed to be searched it would be clear I'm making youtube videos.. and nothing else 😅

    • @nunyabisnass1141
      @nunyabisnass1141 6 หลายเดือนก่อน

      @@integral_chemistry some of my other fav TH-camrs have been contacted by the FBI lol. Cody, styro...

    • @chemistryofquestionablequa6252
      @chemistryofquestionablequa6252 6 หลายเดือนก่อน

      @@integral_chemistry just don’t say you have the stuff to make anything scheduled “just in case”, DEA will get you for constructive intent. It’s a bit different with energetics because you’re allowed to make them, just can’t store, transport, etc.

  • @Slavicplayer251
    @Slavicplayer251 6 หลายเดือนก่อน +1

    why is acetone and toluene on the list here in aus you can buy a 55 gallon drum of the stuff no questions asked

    • @integral_chemistry
      @integral_chemistry  6 หลายเดือนก่อน +1

      I've actually got no idea.. I know acetone because it's just such a broadly useful solvent and maybe that's true for toluene as well? I know you can use both to make other chemicals that are one step closer to controlled compounds, but you could apply that logic to literally anything. Styrofoam is just a few simple steps from multiple controlled compounds, easy enough for any graduate chemistry student. That's why the whole concept is preposterous for individuals in terms of the scope of what constitutes "precursor".

    • @Slavicplayer251
      @Slavicplayer251 6 หลายเดือนก่อน

      @@integral_chemistry it may be because toluene is the precursor to tnt

  • @NonyaBiz-t5f
    @NonyaBiz-t5f 5 หลายเดือนก่อน

    idk which smell i like more: fresh made methlamine or oxidatively cleaved tryptamines. fish or poop, choose wisely.

  • @LogieD223
    @LogieD223 6 หลายเดือนก่อน

    Welcome to the watchlists everyone!

    • @AtlasReburdened
      @AtlasReburdened 6 หลายเดือนก่อน +1

      Lol, welcome, good one.

  • @druidplayz2313
    @druidplayz2313 5 หลายเดือนก่อน +1

    Waltah we dont need the barel walta

  • @samuelbright8713
    @samuelbright8713 6 หลายเดือนก่อน +3

    I like dragons

  • @GiftedPoultry528
    @GiftedPoultry528 5 หลายเดือนก่อน

    Next video: Making methamphetamine with the methlyamine I made.