Converting yellow palladium salt (Palladosammine Chloride (NH3)2PdCl2) ) to palladium black and melting it into a button. #owltech #palladium #preciousmetals Music: / awc6f
@OwlTech333 of course, it's so hard to get nice Pd sometimes but I will have to try the borax to stop oxidation as it's cooling trick I just learned from this video. Thanks
@@OwlTech333 شكراً للرد …. لكن اسمح لي بالتوضيح اكثر من بعد اذنك … قمت بإضافة ماء ساخن إلى إحدى العينات الترابية و بعد الفلترة وجدت أن الماء قد انصبغ باللون الأصفر .. فقمت بتبخير الماء و وجدت اني قد تحصلت على ملح اعتقد انه ملح البلاديوم . سؤالي الان هل فعلاً من الممكن ان يذوب ملح معدن البلاديوم بالماء فقط بهذه الطريقة ؟؟؟ و هل اذا كلست هذا الملح بعد تبخير الماء عنه يكون قابل للصهر ؟
No specific ratio used, just after adding the formic, add the NaOH on small increments, waiting to react between additions until all yellow salt turns black, then continue boiling for 5-10 minutes and it’s done. You don’t need much reagents - for this reduction I used roughly 50ml formic and 10-15g NaOH
Do you prefer NaOH vs NH3? And which Salt reduces quicker with Alkaline/formic acid, Yellow or Red Brick? I had some delayed issues yesterday reducing ~30 grams of red salt with HN3/Formic Acid. Seemed either not enough heat at first or my NH3/formic solution was to diluted.
Sir how are you I have ground many stones and dissolved them in Aqua Regia (stones with stannous chlorid test show Platinum group metals) after urea adding SMB and some Iron sulphide ten grams dust was received around I once again made Aqua Regia to make pure gold, half of the dust did not dissolve, I do not understand what metal it could be.
Hello, good evening, my name is Diego, I'm from Brazil. do you have email so i can send some questions ?? for example: I have an ammoniacal solution containing palladium .... I added hcl and yellow pd salt precipitated .... IF I TAKE THAT YELLOW SALT AND ADD FORMIC ACID AND THEN GO PUT IN SODIUM HYDROXIDE, WILL IT BE BLACK LIKE THIS ?? .....I WORK WITH RHODIUM, PALLADIUM, GOLD AND SILVER ....IT WILL BE A PLEASURE TO EXCHANGE INFORMATION. HUGS
@@OwlTech333 aww! HTe it when it gets away from us for cheaper than value! I remember when palladium was 10% what platinum was. It was like copper or maybe silver. Now platinum is palladium's junior league metal, like silver is gold's... anyways. Just curious.
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Fantastic quality of the refining and melt! 🌟🌟🌟🌟🌟👍
Thank you!
Здоров дружище! Красота!
Спасибо большое!
شكرا لك استفدنا منك ❤❤❤
Залипательное видео, приятно видеть как работает маэстро.
Спасибо за просмотр!
👏👏
Отличная работа!
Спасибо!
Beautiful piece mate 👌
Glad you like it!
@OwlTech333 of course, it's so hard to get nice Pd sometimes but I will have to try the borax to stop oxidation as it's cooling trick I just learned from this video. Thanks
Привет, красивая палладиевая чернь получилась.
👍
Привет! Спасибо!
Very good videos,thank You Owl Tehc.👍🤗👍
Glad you like them!
Nice.. Pd is very unique.. sometimes , i feel that palladium metal is alive😅 they expand sometimes. Like a metal sponge
Very cool glad to see you back😊
More to come!
جميل جدا جدا روعه تسلم استاذ العزيز بلتوفيق أنشاء آلله تحياتي يا من مصر
Thank you!
Beautiful dude!
Score 👍
Peace Prospector Tripp
Thanks 👍
Top você realmente mostra como se faz, parabéns 👏👏👏👏
So beautiful video I like it❤❤❤
Good job you prof thanks for video
Thanks for watching!
Professionnel thanks for vidéo
iridium please...
Отличная работа👍 раньше плавил без буры или я ошибаюсь?
Спасибо! Тоже с буры плавил
@@OwlTech333 Я палладий плавлю с содой Na2CO3
مرحبا اخي فيديو رائع اخي هل ينطبق الامر على البلاتين كذلك بعد ترسيب ب كلوريد المونيوم التحويله الى اكسيد جاهز الصهر لك شكر وتقدير ❤
Ok
thanks for goood video patron 🌹🌹🌹🌹👍
Thank you for watching!
Rất hay! Cảm ơn bạn!
Hello, greetings to you for the wonderful effort, sir. I have a group of platinum mixed with sand, which is chloride. How do I start working on it?
Hello, very good job!
I am converting the yellow salt using HCL and zinc, have you ever tried it?
Yes
سؤال لو سمحت …
هل يذوب ملح البلاديوم بالماء فقط ؟
و هل اذا كان يذوب فطريقة تحويله الى معدن هي نفس الطريقة في هذا الفيديو ؟
يمكنك تحويل ملح البلاديوم إلى معدن بطريقة تسمى التكليس، لكني أفضل التحويل الكيميائي باستخدام حمض الفورميك.
@@OwlTech333 شكراً للرد ….
لكن اسمح لي بالتوضيح اكثر من بعد اذنك …
قمت بإضافة ماء ساخن إلى إحدى العينات الترابية و بعد الفلترة وجدت أن الماء قد انصبغ باللون الأصفر .. فقمت بتبخير الماء و وجدت اني قد تحصلت على ملح اعتقد انه ملح البلاديوم .
سؤالي الان هل فعلاً من الممكن ان يذوب ملح معدن البلاديوم بالماء فقط بهذه الطريقة ؟؟؟
و هل اذا كلست هذا الملح بعد تبخير الماء عنه يكون قابل للصهر ؟
Hi.What are the ratios of formic acid and sodium hydroxide?
No specific ratio used, just after adding the formic, add the NaOH on small increments, waiting to react between additions until all yellow salt turns black, then continue boiling for 5-10 minutes and it’s done. You don’t need much reagents - for this reduction I used roughly 50ml formic and 10-15g NaOH
لو سمحت يافنان الفيديو نازل من غير ترجمة من فضلك اعد صياغة الفيديو بالترجمة
فيديو رائع
Здравствуйте!
Отлично!
Скажите, какую музыку используете в ролике?
Спасибо! Музыка моя: on.soundcloud.com/awc6F
Hi Mr owl, good?
The yellow salt is come from? Please.
MLCCS
Do you prefer NaOH vs NH3? And which Salt reduces quicker with Alkaline/formic acid, Yellow or Red Brick? I had some delayed issues yesterday reducing ~30 grams of red salt with HN3/Formic Acid. Seemed either not enough heat at first or my NH3/formic solution was to diluted.
Hi! Prefer NaOH, never reduced the red salt before so I don't know. As for you issues, heating to at least 85C is a must.
Sir how are you I have ground many stones and dissolved them in Aqua Regia (stones with stannous chlorid test show Platinum group metals) after urea adding SMB and some Iron sulphide ten grams dust was received around I once again made Aqua Regia to make pure gold, half of the dust did not dissolve, I do not understand what metal it could be.
😑 why did speed up the video when melting! How much didt tooked?
5min
@@OwlTech333 i melted palladium in less than one minute with arc but the carbon electrodes are a mess. Now i have rhodium 🤞
سلام عليكم عندي بلاديوم اصفر كيف تحويله الئ بلاديوم هل ضيف عليه نتريك ام ماذا ارجو الرد
With formic acid
Qual foi o processo para obter o sal amarelo de paládio
There’s a video
Very nice button!
I couldnt see the weight... ill guess maybe a little high, around 11g.
Great vid OwlTech.
9.48g
@@benlee4940 thanks.
9.48g Thank you!
سلام عليكم اخي العزيز اذا كان يوجد في الماء الملكي رصاص كيف التخلص منهو
H2SO4
@@OwlTech333 اخي العزيز ألم افهم
ما برای کار کردن به چه صورت بفهمیم که فلز ما رادیوم هست ممنون میشم
Black paladio l thinkso l gotte sir,
16 👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍
Спасибо!
Озвучка повний пізд**.
Дякую за відео
Sir after is black color
What do you mean?
@@OwlTech333 sir when you finish litle be more late paladio is lite be more dark
Hello, good evening, my name is Diego, I'm from Brazil. do you have email so i can send some questions ?? for example: I have an ammoniacal solution containing palladium .... I added hcl and yellow pd salt precipitated .... IF I TAKE THAT YELLOW SALT AND ADD FORMIC ACID AND THEN GO PUT IN SODIUM HYDROXIDE, WILL IT BE BLACK LIKE THIS ?? .....I WORK WITH RHODIUM, PALLADIUM, GOLD AND SILVER ....IT WILL BE A PLEASURE TO EXCHANGE INFORMATION. HUGS
Yes it should be exactly as this
Това е завотско рафиниране така се рафинира в целият свят точно така го правя и аз
Bravo!
След амоняка го въстанивявам с солна при пеха 2
И накуя ты его плавил?? Не проще ДОРЕ получить отправить на завод за 5 % на афинаж?? Куда отработку деешь?? Соседям по даче сливаешь))
нет, не проще
@@OwlTech333 Лицензия есть на драги?
How much would you sell that little button for? Have you given thought to opening a store or do you have one already?
This one was sold the same day it was made. Unfortunately it went for 20% below spot price
@@OwlTech333 aww! HTe it when it gets away from us for cheaper than value! I remember when palladium was 10% what platinum was. It was like copper or maybe silver. Now platinum is palladium's junior league metal, like silver is gold's... anyways. Just curious.