Locking and Shimming

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  • เผยแพร่เมื่อ 12 มิ.ย. 2017
  • Here we look at some of the ways we try to maximize the power of NMR, in processes called locking and shimming.

ความคิดเห็น • 17

  • @AlphaNumeric123
    @AlphaNumeric123 3 ปีที่แล้ว +6

    Absolutely fantastic teacher. He strikes the balance between making something accessible and--importantly--intuitive while also not watering things down too much or simplifying to the point of distortion. Really has the touch of a professor as opposed to a TH-cam educator, which I mean as a compliment. Sub'ed and look forward to looking at more content!

  • @Brsawesome
    @Brsawesome 2 ปีที่แล้ว +4

    Hi Jeff, great explanation. Only 400 MHz, is 400 million Hertz (rather than 400 billion Hertz). Keep up the good work!

  • @vanfidel
    @vanfidel 6 ปีที่แล้ว +8

    Great explanations, thanks. Cracked me up how disgusted you looked about it looking like a UV spectrum.

  • @seamus9898
    @seamus9898 2 ปีที่แล้ว +2

    awesome! best video I've found on lock & shim

  • @RohitPant04
    @RohitPant04 ปีที่แล้ว +2

    Well done, Jeff. This was well presented!

  • @ramjayakumarv9934
    @ramjayakumarv9934 2 ปีที่แล้ว +2

    Great explanation sir. Thank You.

  • @enzolong9085
    @enzolong9085 2 ปีที่แล้ว +1

    Really cannot thank you enough for this explanation sir. Bless you

  • @Pepsimaximo1
    @Pepsimaximo1 2 ปีที่แล้ว +1

    Great explanation, thank you

  • @matiafossatti9091
    @matiafossatti9091 3 ปีที่แล้ว +1

    Great explanation, many thanks, prof. Jeff.

    • @jefforvis461
      @jefforvis461  3 ปีที่แล้ว +1

      Thank you, I appreciate it.

  • @aag7274
    @aag7274 6 ปีที่แล้ว +2

    very helpful
    thanks Jeff

  • @alcevallo4631
    @alcevallo4631 2 ปีที่แล้ว +1

    Thanks!

  • @Phosphoenol_pyruvate_CK
    @Phosphoenol_pyruvate_CK 2 ปีที่แล้ว +2

    Hi. Please I am wondering how long does it take to acquire a spectra from a sample on standard NMR machines?

    • @jefforvis461
      @jefforvis461  2 ปีที่แล้ว +2

      The answer is ... it depends. A standard proton spectrum of a reasonably concentrated sample can be acquired in under a minute. A highly dilute sample that requires over 100 scans can take five minutes. If one were to do a whole suite of experiments on a sample (proton, carbon, DEPT, COSY and so on) at least an hour of time is usually required.
      The longest experiments we typically see are carbon spectra of samples that have a low solubility in any common deuterated solvent. Those can be overnight runs of thousands of scans to get well defined peaks and a reasonable signal to noise ratio.
      I hope this helps.

    • @Phosphoenol_pyruvate_CK
      @Phosphoenol_pyruvate_CK 2 ปีที่แล้ว +1

      Thank you

  • @nowar6697
    @nowar6697 4 ปีที่แล้ว +2

    Very well explained
    Jeff Orvis, i think it is 4bn instead of 400bn. lovely lecture