Hey, I can suggest one more way to separate the compound: You can dissolve it in concentrated sulfuric acid in order to isolate the carbocation. Then, carefully rehydrate the carbocation by pouring the mixture into ice water. Triphenylmethanol will precipitate out, and you can filter it.
Greak work! I am running this experiment tomorrow in my organic chemistry lab but on a smaller scale. It was really insightful to see the reaction performed with different equipment and synthesis techniques!
Great video! At 4:25 on the top left corner there's a mistake on the text box, it should say "30 ml of a 10% solution of sulfur acid was made..." Instead of "30% solution of sulfur acid was made...".
Hey Vibzz nice video! Grignard reactions are always fun to watch. Could you please display the molar equivalents also? Not only just grams. This helps actual chemists on scaling procedures, modifications and mechanistic understanding.
Add more sulfuric acid and the TPM will not crash out. If you then dilute the flask contents into acidic ice water, the TPM will crash out. Just might make your yield a bit better
@@vibzzlab but even dry is not completely dry afterall u are living in a coastal area there will always some moisture content. But good to see it went successful but a drying tube with silica gel or molecular sieves could have been also used instead of CaCl2
I wonder what that could be a catalyst for.. here's a homework assignment for you: A FOOD SAFE GLOW IN THE DARK DRINK ADDITIVE. HINT: SHAKE IT TO CAUSE THE GLOW😘
@@vibzzlab the world is ready for glowing food. See if you can find them. Peanut butter does, but i mean wayyy better ones coming (heres a hint: singlet oxygen, shaking or swirling the bottle and drinks)
Hey, I can suggest one more way to separate the compound:
You can dissolve it in concentrated sulfuric acid in order to isolate the carbocation. Then, carefully rehydrate the carbocation by pouring the mixture into ice water. Triphenylmethanol will precipitate out, and you can filter it.
Greak work! I am running this experiment tomorrow in my organic chemistry lab but on a smaller scale. It was really insightful to see the reaction performed with different equipment and synthesis techniques!
Nice work!! 👍👍
Thank you and glad to see you back in action :)
@@vibzzlab Thank you! 🙂
"Since it was so late I went to sleep" 😂😂 relatable
Great video!
At 4:25 on the top left corner there's a mistake on the text box, it should say "30 ml of a 10% solution of sulfur acid was made..." Instead of "30% solution of sulfur acid was made...".
Hey Vibzz nice video! Grignard reactions are always fun to watch. Could you please display the molar equivalents also? Not only just grams. This helps actual chemists on scaling procedures, modifications and mechanistic understanding.
I'll do that from future videos 🙂
Yes thank you
Add more sulfuric acid and the TPM will not crash out. If you then dilute the flask contents into acidic ice water, the TPM will crash out. Just might make your yield a bit better
Good to see u doing grignard reaction but I couldnt see a drying tube above the condensor
I didn't use it. It will be much better if you can place one on top
@@vibzzlab but why and how did the reaction go smooth because the place where u live is humid
@@akhilthechemist it was dry since 1 month. So I decided to give it a go. I had been waiting for months for this opportunity
@@vibzzlab but even dry is not completely dry afterall u are living in a coastal area there will always some moisture content. But good to see it went successful but a drying tube with silica gel or molecular sieves could have been also used instead of CaCl2
I’m actually running this exact reaction tomorrow in organic chemistry lab course. Great work!
Thank you for your support
gj as always, heres one for the algo
New intro also nice
Thank you
Nice work!!!!!❤️
Thank you
😊
Hm, I've never even heard of this compound before. Very interesting though.
nice job
Thank you
Cool
I wonder what that could be a catalyst for.. here's a homework assignment for you: A FOOD SAFE GLOW IN THE DARK DRINK ADDITIVE. HINT: SHAKE IT TO CAUSE THE GLOW😘
Didn't quite get you
@@vibzzlab the world is ready for glowing food. See if you can find them. Peanut butter does, but i mean wayyy better ones coming (heres a hint: singlet oxygen, shaking or swirling the bottle and drinks)
Are you indian ?😅
Ofcourse
Good explanation sir😁💐
Nice
Thank you