Bruker D2 Phaser required training for MCL

This video shows the Bruker D2 Phaser's setup in the Materials Characterization Lab at the University of Utah. It goes over the setup and operation of the machine, and is required as a first step for those wishing to use the machine in the lab.
*This video was created with the sole intent to train clients of the MCL in the proper use and standard operating procedures used in the lab. It does not represent the views of the machine's manufacturer or any other party.

[@sercho0o]

Do you have any guide for the finding peaks options? Great video, thanks

[@materialscharacterization4168]

Hi, glad you liked the video! I'm not sure I know what you mean by "finding peaks options." If you mean analysis software that can identify the peaks and do matching, we use Match! Crystal in our lab. We have used HighScore Plus in the past. There are many other options, though, that range from expensive to free. GSAS is a common one that our students use. It's free, but requires some python programming knowledge.

[@siowhwateo2205]

Before analyzing the sample, did you calibrate the instrument in terms of peak position?

[@materialscharacterization4168]

I know most XRD machines have the capability to calibrate the instrument, but I'm not familiar with the procedure for doing so on the D2 Phaser. We do regularly run a NIST Si line standard (every 3-4 months) which we use to calculate the offset of the instrument. The D2 Phaser remains pretty consistent from month to month.

[@jhoeldarwinchoquehuancapom2605]

HELLO, I NEED THE USE MANUAL FOR THE PASHER D2 EQUIPMENT, I WOULD APPRECIATE YOUR ANSWER.

[@materialscharacterization4168]

Hi, our D2 Phaser came with several manuals ranging from quick start guides to more in-depth maintenance and operation procedures. May I ask what the manual is needed for? Is this something you've already contacted Bruker about without success?

[@marasini]

can you do the same in clay samples

[@materialscharacterization4168]

We have done some clay samples in our XRDs. Collecting data for clay is rather simple. However, clay can contain several completely separate phases which overlay and make phase identification (not included in this video) rather complex. There are some procedures out there to help isolate certain phases. Google searching "Clay separations for XRD" can give you some good starting resources.