Are you interested in the progress, that led to this point? If so, you can check out the cesium Playlist: th-cam.com/play/PLLERbxERv6_9Q71ruVQsF1KMmMFUERcs2.html Do you want to see potassium being distilled? th-cam.com/video/Y7YdT-vavHQ/w-d-xo.html
I just randomly found one of your videos today, you now have a like and a subscription and new fan. I wish to make a 'Jacobs Ladder' and I found your video when you made a 50k voltage device by using 24v supply and a flyback device, that was some very fine work indeed. I hope to make a small Jacobs Ladder in a sealed container as a novelty toy for a friend of mine. I would like to keep the size relatively small, like an Executive Toy that could sit on his office desk, any advice would be greatly appreciated. Peace and best wishes from Ireland mo chara.
In the pharmaceutical industry we'd call that an ampoule, before and after sealing. A vial is a glass container sealed with a stopper, usually made of some type of rubber.
@@AdvancedTinkeringdude your accent tells me that you’re german so the word „Ampulle“ should be the first thing that’s coming to your mind when you see that thing 😅
I have no clue what someone would want this amount of pure caesium for but good lord. The sheer guts you have to remove the flasks not once, but twice- without wearing gloves or anything, floors me. Please stay careful, man. This is basically elemental napalm
Gloves aren't of much use if you're handling materials that will not only end your day but also close the lab/the building/the area indefinitely if you drop them...
I'm not a scientist by any means but watching this I can't but be curious as to what kind of reaction you could get if you were to submerge one of the ampuls deep enough for glass tube to collapse under the water pressure. I imagine it wouldn't have to go too deep considering the glass is already a vacuum so adding more external pressure (again I'm not a scientist but from my understanding that would mean that the glass only receiving pressure from the outside) so I guess the questions that come to mind are how deep would it have to go to have a catastrophic failure, and what kind of reaction would happen/ be visible/ observable from the surface
@@d0h depends on they type but initially only the outermost layer of caesium would react. It would be a potentially survivable explosion but your hands are gone if you're not using idk, 5mm kevlar gloves or smth. Furthermore, that's pretty much a glass frag
@@michealrollins6656 It really depends on the thickness of the ampule. And I think it's safe to say he's not storing his cesium in something as thin as one of the old smelling salts poppers. It might be strong enough that when the glass fails, you'll only get a few bubbles of hydrogen and oxygen at the surface. Maybe with a wisp of reaction product fumes in them.
The fact that metal can be distilled from a solution in the same way alcohol can is amazing to me. It’s metal in a liquid state so I guess it’s not THAT counterintuitive but I suppose I just never thought about this before. Really neat,thanx!
yeah distillation of metal is pure insanity to me, since its a metal i instantly picture it as one of the hardest solids possible, then we have this "metal" thats just chillin in liquid form and decides to become cloud at high enough temp
@@FreelancerFreak i went to public school, our chemistry class was basically a room of 4 burnouts , the quirky girl who was just "misunderstood" and pair of pregnant besties that spent the entire class comparing due dates. Edit: ooo, and I almost forgot about Ms. Seaton.. she was the teacher...something about the way she would come over to my desk and just stare me down with her fiery yet disappointed stare from behind her half scrip glasses... She would cross her arms in that ugly little sweaty vest and just shame me for slacking off... I loved it. Anyways, what were we talking about?
I've been looking for high-purity Cesium everywhere and I just can't find any! I LOVE how clean this looks! I'll pay you to make some for meeee! Seriously!
That lampwork is not trivial, well done! Based on the quality of your work I think you've probably seen this trick before, but I want to encourage you to try cracking off tubestock with the hot tip of a glass rod instead of the torch and water method. It'll take you a couple tries to dial in how much hot you want for the weight of tubing, but once you do I think you'll find it easier to avoid those spiderwebs you get the way you're doing it. No water, just touch a hot rod onto your score and hold it there til it cracks. When your heat is right for a clean break, that's a good 2-10 seconds, longer than you'd expect. Sometimes they even go 30 seconds later as they're naturally cooling down. The key advantage to this method is you get to control both the temperature of the glass rod, and how much mass of glass you heat up to deliver x heat at y rate.
What really rips a hole in my mind is that there was a first person ever that discovered the process of how to do this. I can not wrap my head around how that idea would even manifest itself, and then formulating a plan to create a previously unknown substance out of nothing. It's so fascinating
I would call myself a multipurpose talent in different topics like mechanics, electronics and software. But chemistry is one of those topics i barely get the basics. Anything above that is magic for me.
I used to be a lampworker and my chemistry is lacking, but this was amazing to watch. Good job keeping yourself safe, that procedure is something i could never do out sheer fear. Chemistry is beautiful and thanks for showing the distillation footage never seen liquid metal be distilled. Do you ever worry about the stress the glass is under when you're heating it up during the distillation
I see the glassware meant to be melted together all the time, but I've neither ever used it or ever even seen it used untill your video. You are very skilled at it. The closest I've even done is making ampuals out of large test tubes by heatingnand stretching the top to a thin tube, filling it, then sealing it. I used them for Bromine, which there is no other way i know how to store safely and not get cancer or poisoned due to it leaking or exploding. I tried vials with rubber stappers crimped on with metal, but is failed greatly. Luckly i left it outside.
No idea how this video got into my recommended box, but i like it. Watching the cesium condensate on the glass walls just to vaporize instantly when you go over it with the flame, just doesn't seem right for a metal xD I love the final shot with the crystallized blobs in the vial. Melting point of 28,44°C, so it's mostly solid when sitting on the counter, but melts in your hand. That's so cool.
That little bit of reactivity you spoke of when you disconnected the stainless steel tube would have been something I would have liked to see. Feel free to add moments like that to the video. It is an important part of the learning and understanding process.
The stuff is fairly easy to make considering how reactive it is. Refining cesium salt and containing it in a glass tube is 2 different things. Potassium Metal was scary. Even small pieces will light up when reacting with organic matter.
I can’t get enough of watching this video, cesium is one of my favorite alkali metals along with rubidium and potassium given that we can easily see it as a gorgeous shiny metallic liquid as it melts at a reasonably low temperature unlike say sodium which needs something like boiling water in order to melt.
A nice thing to have is an oxygen sniffer to ensure full purge . Very cheap to buy and quite surprising when you first get one when you see how the purge takes place in the different setups. Thanks for your videos man it's fun to watch ❤
I don't see any problem there. That's standard practice. Good luck sealing a borosilicate glass vial properly without an propane/oxygen torch ;) And what would the gloves be useful for? Gloves that would protect you from burning cesium would decrease your dexterity too much and thus increase the risk of accidents.
I've been following your journey for some time, and this is an incredible culmination to your skill and dedication. Congratulations! Amazing and joyful science.
That is absolutely gorgeous!!!!!!! What a satisfying feeling to watch it!!! Never thought I would say that about cesium but there it is😂 I would stare at it a lot if I had some of that beautiful substance
It really is the most beautiful stuff. Like, can you imagine showing this to 17th-century alchemists? They'd think you'd discovered the elixir of life.
started maniacally laughing as soon as i saw the ampoule cause i instinctively felt the amount of blood, sweat, and tears poured into making such a terrifying thing
i managed to make a shiny 5mm drop of shiny sodium in an ampule made from a pipette, just put it in and melted the sodium several times and made it consume all the oxygen, once it stopped tarnishing anymore i could melt it and roll it to the other side of the test tube and then shortened the tube, was quite happy with the results and then i see you do this haha
I melted some sodium hydroxide in a nickel crucible with a sprit flame and electrolysed it with a car battery, the sodium would gather around the electrode and could be collected. The current was 12A. Do not spill the molten sodium hydroxide. My friend spilt some on a notepad and it ate straight through the thick pad of paper instantly. I tried potassium hydroxide but it didn't work. I read that the potassium dissolves in the hydroxide, not sure if this is the case.
I dont think even Applied Science (basically a genius, to me, also) could pull this off I'm not aware if he possesses the glass skill you have.. Absolutely fantastic work thank you for sharing!
Ben from Applied Science if without a doubt a genius. I am pretty sure that, if he would really try and learn/practice some glass blowing, he would be able to do it. But thank you a lot for the compliment!
Before you said it was cesium, I thought it was just mercury. I had a much larger and more precariously contained stash of mercury when I was a kid. My dad would remodel apartments and hotels, and one of my jobs was to remove all the thermostats. I'd gather up all the mercury switches, and dump them in bucket. It was like a 1/4 of the way full before the sides started to bulge. My mom made me surrender it to the university because she was afraid I was going to spill it and poison the water supply.
Absolutely amazing work! Cs has a boiling point of 690 °C under normal pressure. Do you have an idea, at which temperature this stuff distilled over at your low pressure?
Incredible! Cesium is definitely my favorite element, I read that there is an alloy of sodium potassium and cesium which melts at -79 degrees. You song see many channels dedicated to such reactive elements!
Are you thinking about purifying the potassium metal shown in one of your recent videos using this same exact distillation method? BTW cesium is one of the most gorgeous looking elements of the entire periodic table!! I would love to get my hands on some cesium metal especially on some at such high purity that it won't adhere to the glass at all when melted, sucks that a gorgeous golden colored metal that can be melted easily is incredibly pricey and dangerously reactive. 😞😞😞😞😞😞
Yes, I am currently working on distilling potassium to get a large clean vial. But I also want to make the potassium myself. Yes it definitely is beautiful :)
What I think is impressive is that the Cs doesn't stick AT ALL to the glass. I have a 5 gram ampule of 99.95 purity from a respectable chemical lab supplier (hasn't broken in 20years thank God!) and it sticks just a little especially at the tip where the glass was sealed. And it has a concave meniscus, which indicates some albeit redicilously little contamination... But yours flows almost like Hg. The inside glass must be VEEEERY clean. Amazing how just the slightest impurities can mask the true nature of materials. Our vast semiconductor industry and by extrapolation our digital age would be impossible if we were only able to achieve 99.99% purity... An operation room is a pig sty in comparison to a semiconductor factory. Good craftsmanship!!
Holy shit! 👏👏👏👏👏 Dude, this was my first video of yours and it was awesome, I loved it, Fantastic work on the project and the video and how fucking cool is that insane pattern thing it’s doin inside the glass, that’s incredible!! Did You not geek out over that? Now I’m off to binge the rest of your work, I bet it’s all gonna be just as incredible! 🙏🏼 Really appreciate You Man!
Beautiful video! What do you recommend for storing a cesium ampule at home? I was thinking about a steel box with a larger amount of sand surrounding the ampule. Any better or additional ideas for safety?
Thank you! Yes, I think an airtight steel box with some PE foam with a cutout for the vial would be best. So even if the box gets knocked over, the vial will be likely to survive. With sand it would be more likely to break. Just make sure the foam does not react with the cesium, otherwise pressure could build in the box if the vial breaks and gaseous reaction products are formed.
Thanks for the reply. Do you have a recommendation of a commercial polymerfoam with these properties (maybe even a supplier)? My reasoning with sand was that the cesium reacts with sand and gets quenched rather than being oxidized in air and starting a fire.
The cesium would not react with the sand in my experience. Of the steel box is airtight, I don't think it would start a fire, there just not enough oxygen. There are a lot of suppliers of polyethylene foam on the internet. In my experience PE will not react with cesium.
I thought about that. But no. As you can see, the amount of cesium that condensed even at the very beginning of the stainless steel hose is minute. In addition I bent the hose in a circle so cesium atoms making it into the hose would have to hit the walls and condense on their way to the pump.
Is it possible to use an induction coil to hear the ceasium? That would allow potentially fine control over the heating rate, and avoid over heating the glass.
This process looks dangerous. I imagine seeing this hundreds of years ago would look like magic. The level of skill makes you like a magician. Nice job.
I know very little about the world of chemistry and in particular the metals like this that are most amazing but I can say for certain fear of mercury is nothing after seeing this stuff!
Wow 🤩 this is truly amazing! I clearly have no clue what is going on, but this is one cool project! Science is so fascinating! Love this and glad I have found this channel!!
That's some high level shit. Your channel is underrated. Damn from the technical view this is the same level as chemicalforce. You could improve a little with the video editing but damn this is so impressive from the technical view.
Thank you! Yes, there is a lot of improvement when it comes to editing and filming. But it's always hard to film when you are alone and busy working on something.
Are you interested in the progress, that led to this point? If so, you can check out the cesium Playlist:
th-cam.com/play/PLLERbxERv6_9Q71ruVQsF1KMmMFUERcs2.html
Do you want to see potassium being distilled?
th-cam.com/video/Y7YdT-vavHQ/w-d-xo.html
Is this something that the CIA, FBI will come after you ?
I just randomly found one of your videos today, you now have a like and a subscription and new fan. I wish to make a 'Jacobs Ladder' and I found your video when you made a 50k voltage device by using 24v supply and a flyback device, that was some very fine work indeed. I hope to make a small Jacobs Ladder in a sealed container as a novelty toy for a friend of mine. I would like to keep the size relatively small, like an Executive Toy that could sit on his office desk, any advice would be greatly appreciated.
Peace and best wishes from Ireland mo chara.
I would! I would also like to see a video of you making rubidium.
This is golden alchemy for real. ❤
Are you going to open it?
The cesium crystals and distillation footage is so mesmerizing... absolutely fantastic work!
Thank you!
most dangerous object I've held in my hands was my d*ck lol
It's like bismuth and mercury had a baby... a baby who hates the world...
@@arbodox AND good music, too!!
In the pharmaceutical industry we'd call that an ampoule, before and after sealing. A vial is a glass container sealed with a stopper, usually made of some type of rubber.
Yes I think that's the correct term. Took me some time to get the English terminology right.
I call that, a uh, exotic glass bauble son.
would not a glass stopper also count?
@@AdvancedTinkeringdude your accent tells me that you’re german so the word „Ampulle“ should be the first thing that’s coming to your mind when you see that thing 😅
@@rolux4853 considering an ampoule is a sealed vial... 🤷♂
both are correct
My heart was in my mouth when you were sealing the ampoule, respect sir that’s a great project 👍🏻
Thanks, I appreciate the compliment! If you liked the ampoule being sealed, I can recommend my video about the Potassium distillation ;)
why anyone would want to skip the precipitation process is beyond me. its the best part. just beautiful!
I have no clue what someone would want this amount of pure caesium for but good lord. The sheer guts you have to remove the flasks not once, but twice- without wearing gloves or anything, floors me. Please stay careful, man. This is basically elemental napalm
Wouldn't it be more comparable to white phosphorus than to Napalm? I think the reaction you're talking about would be very similar to W.P.
Gloves aren't of much use if you're handling materials that will not only end your day but also close the lab/the building/the area indefinitely if you drop them...
I'm not a scientist by any means but watching this I can't but be curious as to what kind of reaction you could get if you were to submerge one of the ampuls deep enough for glass tube to collapse under the water pressure. I imagine it wouldn't have to go too deep considering the glass is already a vacuum so adding more external pressure (again I'm not a scientist but from my understanding that would mean that the glass only receiving pressure from the outside) so I guess the questions that come to mind are how deep would it have to go to have a catastrophic failure, and what kind of reaction would happen/ be visible/ observable from the surface
@@d0h depends on they type but initially only the outermost layer of caesium would react. It would be a potentially survivable explosion but your hands are gone if you're not using idk, 5mm kevlar gloves or smth. Furthermore, that's pretty much a glass frag
@@michealrollins6656 It really depends on the thickness of the ampule. And I think it's safe to say he's not storing his cesium in something as thin as one of the old smelling salts poppers. It might be strong enough that when the glass fails, you'll only get a few bubbles of hydrogen and oxygen at the surface. Maybe with a wisp of reaction product fumes in them.
The fact that metal can be distilled from a solution in the same way alcohol can is amazing to me. It’s metal in a liquid state so I guess it’s not THAT counterintuitive but I suppose I just never thought about this before. Really neat,thanx!
I watched the thought Emporium (I think) make silver by shining UV light on an viall containing a silver solution.. it's magic! 😁👌🏼
There is something very disturbing yet beautiful about watching a metal be distilled. It seems like something that should not be possible.
I mean, its a liquid at room temp. Where did this metal come from? I agree with you, this is wild.
Chemistry is amazing.
@@MattShine11_pure_ caesium is liquid at or near room temperature. It's found in Pollucite ore and primarily mined in Canada.
yeah distillation of metal is pure insanity to me, since its a metal i instantly picture it as one of the hardest solids possible, then we have this "metal" thats just chillin in liquid form and decides to become cloud at high enough temp
We do it with water all the time, tho that's technically more like a mineral when it's solid
I will not lie, i have no idea what i just watched or what you just made, or even what its for, but it was beautiful.
Believe it or not, atomic clocks
@@lancehiggins828 explosive atomic clocks sounds pretty cool
@@lancehiggins828No thats Cs137
This is stable cesium
How do you not know what cesium is? Didn't you take chemistry in school?
@@FreelancerFreak i went to public school, our chemistry class was basically a room of 4 burnouts , the quirky girl who was just "misunderstood" and pair of pregnant besties that spent the entire class comparing due dates.
Edit: ooo, and I almost forgot about Ms. Seaton.. she was the teacher...something about the way she would come over to my desk and just stare me down with her fiery yet disappointed stare from behind her half scrip glasses... She would cross her arms in that ugly little sweaty vest and just shame me for slacking off... I loved it.
Anyways, what were we talking about?
Amazing, cesium is so beautiful.
I've been looking for high-purity Cesium everywhere and I just can't find any! I LOVE how clean this looks!
I'll pay you to make some for meeee! Seriously!
@fbi
It really doesn't come across how utterly dangerous this was. Very cool video.
Imagine dropping the science bath bomb
@@silverblank1139 Most underrated comment I've seen in a long time.
I only have some long past undergrad memories of chemistry, but your craftsmanship and work you put into making this is fantastic. great work man.
Thank you a lot!
This certainly has to be the most beatiful video about cesium on youtube. Great job!
The most dangerous thing I ever had in my hand was a wedding ring.
😂
that’s so funny yet so sad
I’m getting out of mine soon. Turns out I was the loyal one
GOLLUM. GOLLUM!!😂
@@cerrudmanuel 😂😂
beautiful video, i especially liked the blur you put over the cesium bottle for no reason
Just a few words to congratulate you for that beautiful piece of Cesium you achieved with your hard effort and knowledge.
Thank you!
one of the most beautiful things shown on youtube in my opinion
Thank you!
That’s an instant follow, I love beautiful elements and incredible craftsmanship, you delivered both flawlessly.
Appreciate it! I am glad you liked the video!
So, if you drop that bottle, how big an explosion or conflagration are we talkin'?
That lampwork is not trivial, well done! Based on the quality of your work I think you've probably seen this trick before, but I want to encourage you to try cracking off tubestock with the hot tip of a glass rod instead of the torch and water method. It'll take you a couple tries to dial in how much hot you want for the weight of tubing, but once you do I think you'll find it easier to avoid those spiderwebs you get the way you're doing it. No water, just touch a hot rod onto your score and hold it there til it cracks. When your heat is right for a clean break, that's a good 2-10 seconds, longer than you'd expect. Sometimes they even go 30 seconds later as they're naturally cooling down. The key advantage to this method is you get to control both the temperature of the glass rod, and how much mass of glass you heat up to deliver x heat at y rate.
Thank you! Yes, by now I mostly use the hot glass bead method to crack the glass. But nevertheless thanks for the advice!
Hot wire is preferred to a "hot tip of a glass rod" which can have unexpected results.
You're practical skills are second to none and an absolute pleasure to watch. That vial of caesium is mesmerising.
Thank you! I'm happy you enjoyed the video!
What really rips a hole in my mind is that there was a first person ever that discovered the process of how to do this. I can not wrap my head around how that idea would even manifest itself, and then formulating a plan to create a previously unknown substance out of nothing. It's so fascinating
The methods used actually are fairly standard.
There much more scary things than cesium btw.
I would call myself a multipurpose talent in different topics like mechanics, electronics and software. But chemistry is one of those topics i barely get the basics. Anything above that is magic for me.
Never seen such a beautiful vial of Ceasium. Absoluut perfection. Thx for sharing with us
Thanks! It was a lot of work.
@@AdvancedTinkering great job✨✌️
You are amazing!!!!! The fact that you did all this without access to an industrial lab is incredible. I love your video! Good Luck in the future! 🎉🥳💯
I used to be a lampworker and my chemistry is lacking, but this was amazing to watch. Good job keeping yourself safe, that procedure is something i could never do out sheer fear.
Chemistry is beautiful and thanks for showing the distillation footage never seen liquid metal be distilled.
Do you ever worry about the stress the glass is under when you're heating it up during the distillation
I see the glassware meant to be melted together all the time, but I've neither ever used it or ever even seen it used untill your video. You are very skilled at it. The closest I've even done is making ampuals out of large test tubes by heatingnand stretching the top to a thin tube, filling it, then sealing it. I used them for Bromine, which there is no other way i know how to store safely and not get cancer or poisoned due to it leaking or exploding. I tried vials with rubber stappers crimped on with metal, but is failed greatly. Luckly i left it outside.
I have absolutely no understanding of what I just watched but it was incredibly entertaining
The only thing to make this video even better would be the Terminator 2 theme song during the destilation
Dziękujemy.
Du bist echt sooooo krass!!!
Hab mir das Video jetzt zum zweiten Mal in dem Jahr angeschaut. Wahnsinn!
No idea how this video got into my recommended box, but i like it. Watching the cesium condensate on the glass walls just to vaporize instantly when you go over it with the flame, just doesn't seem right for a metal xD
I love the final shot with the crystallized blobs in the vial. Melting point of 28,44°C, so it's mostly solid when sitting on the counter, but melts in your hand. That's so cool.
Beautiful
Thank you!
Most underrated channel ive seen in a while
This hits me right in the feels dude. I harken back to the hours I've spent carefully distilling Diethyl Ether.
That little bit of reactivity you spoke of when you disconnected the stainless steel tube would have been something I would have liked to see. Feel free to add moments like that to the video. It is an important part of the learning and understanding process.
Beatiful, Cesium never ceases to amaze, liquid gold hehe
14:21 - Mesmerizing and Beautiful!!
Kudos
Congratulations on your isolation and purification of the Cs! It looks absolutely beautiful flowing around in that ampoule!
7:36 Really, that's wonderful recordings and downright epic with this background music.
I have no fucking clue what is going on but this is absolutely fascinating to watch the cesium being made.
The stuff is fairly easy to make considering how reactive it is. Refining cesium salt and containing it in a glass tube is 2 different things.
Potassium Metal was scary. Even small pieces will light up when reacting with organic matter.
I can’t get enough of watching this video, cesium is one of my favorite alkali metals along with rubidium and potassium given that we can easily see it as a gorgeous shiny metallic liquid as it melts at a reasonably low temperature unlike say sodium which needs something like boiling water in order to melt.
A nice thing to have is an oxygen sniffer to ensure full purge . Very cheap to buy and quite surprising when you first get one when you see how the purge takes place in the different setups. Thanks for your videos man it's fun to watch ❤
10:30
> Seals off glass vial containing liquid metal that combusts on contact with oxygen
> Using oxygen torch
> WITHOUT GLOVES
I don't see any problem there. That's standard practice. Good luck sealing a borosilicate glass vial properly without an propane/oxygen torch ;)
And what would the gloves be useful for? Gloves that would protect you from burning cesium would decrease your dexterity too much and thus increase the risk of accidents.
The final result looks absolutely stunning, awesome work!
1:12 - "In the same schlenk flask". The accent!
That was some phenomenal stuff, you've become quite the pro with this
I've been following your journey for some time, and this is an incredible culmination to your skill and dedication. Congratulations! Amazing and joyful science.
Thank you! Hope you stay around for further further projects.
This video is pure art, amazing job!
Your accent is exactly the accent I want to hear from somebody explaining this sort of thing. Thank you for the amazing video! ;)
Haha thanks!
This is so beautiful. Humans really are amazing creatures.
Why was the pure Cesium in the final ampule a liquid at the beginning of the video but at the end it was a big solid chunk in the ampule
Due to the different temperatures. Cesium melts at ~28 °C.
@@AdvancedTinkeringawesome thanks for the response and clarifying ! It’s so Very interesting
Caesium is an absolutely gorgeous metal. So beautiful. Also so beautiful because it's so dangerous!
That is absolutely gorgeous!!!!!!!
What a satisfying feeling to watch it!!!
Never thought I would say that about cesium but there it is😂
I would stare at it a lot if I had some of that beautiful substance
I need about a hour of footage of that half solid half liquid gold slowly rotating, for recreational purposes
It really is the most beautiful stuff. Like, can you imagine showing this to 17th-century alchemists? They'd think you'd discovered the elixir of life.
That's the nicest cesium I've ever seen!!
What's cesium? actually pretty interesting to see how it partially crystallizes that's cool!!
started maniacally laughing as soon as i saw the ampoule cause i instinctively felt the amount of blood, sweat, and tears poured into making such a terrifying thing
i managed to make a shiny 5mm drop of shiny sodium in an ampule made from a pipette, just put it in and melted the sodium several times and made it consume all the oxygen, once it stopped tarnishing anymore i could melt it and roll it to the other side of the test tube and then shortened the tube, was quite happy with the results and then i see you do this haha
I melted some sodium hydroxide in a nickel crucible with a sprit flame and electrolysed it with a car battery, the sodium would gather around the electrode and could be collected. The current was 12A.
Do not spill the molten sodium hydroxide. My friend spilt some on a notepad and it ate straight through the thick pad of paper instantly.
I tried potassium hydroxide but it didn't work. I read that the potassium dissolves in the hydroxide, not sure if this is the case.
Very good video and work, and your accent is the cherry on top
Still the best video on TH-cam! Nice job!!
Thank you!
I dont think even Applied Science (basically a genius, to me, also) could pull this off I'm not aware if he possesses the glass skill you have.. Absolutely fantastic work thank you for sharing!
Ben from Applied Science if without a doubt a genius. I am pretty sure that, if he would really try and learn/practice some glass blowing, he would be able to do it.
But thank you a lot for the compliment!
Before you said it was cesium, I thought it was just mercury. I had a much larger and more precariously contained stash of mercury when I was a kid. My dad would remodel apartments and hotels, and one of my jobs was to remove all the thermostats. I'd gather up all the mercury switches, and dump them in bucket. It was like a 1/4 of the way full before the sides started to bulge. My mom made me surrender it to the university because she was afraid I was going to spill it and poison the water supply.
You are aware you were storing it in the worst way possible, it's the vapor that kills you. . .slowly.
Man, I'm sorry about the future dementia...
Never have I seen a blowtorch wielded with such boldness. Props to you sir.
the destillation is beautiful!!! Respect!
Yes it definitely is. Thanks!
Incredible video! High production value, insane idea and final product. Loved it and subbed!
Absolutely amazing work! Cs has a boiling point of 690 °C under normal pressure. Do you have an idea, at which temperature this stuff distilled over at your low pressure?
Thank you a lot! I did not measure the boiling point but I would guess it's somewhere between 300-400 °C.
Like Sully said to Mike Wazowski, “You’re not scary. Not even a little. But you are FEARLESS!” Thank you for sharing an amazing demonstration.
This is some supremely excellent work. I am truly impressed. Well done.
That second distillation was something else.
Incredible! Cesium is definitely my favorite element, I read that there is an alloy of sodium potassium and cesium which melts at -79 degrees. You song see many channels dedicated to such reactive elements!
CsNaK is allready on my to-do list! :)
Definitely perfect soundtrack 👌 🥹
I would be too scared of cracking the glass to do that. Great to watch ( from a distance )
The result is simply stunning!
Are you thinking about purifying the potassium metal shown in one of your recent videos using this same exact distillation method?
BTW cesium is one of the most gorgeous looking elements of the entire periodic table!! I would love to get my hands on some cesium metal especially on some at such high purity that it won't adhere to the glass at all when melted, sucks that a gorgeous golden colored metal that can be melted easily is incredibly pricey and dangerously reactive. 😞😞😞😞😞😞
Yes, I am currently working on distilling potassium to get a large clean vial. But I also want to make the potassium myself.
Yes it definitely is beautiful :)
The final images with the soft crystals are out of this world 🤩
Yes, they do look absolutely gorgeous. I would love to be able to touch them.
@@AdvancedTinkering Glad I got your video in my feed, I subscribed immediately 👍🏻
What I think is impressive is that the Cs doesn't stick AT ALL to the glass. I have a 5 gram ampule of 99.95 purity from a respectable chemical lab supplier (hasn't broken in 20years thank God!) and it sticks just a little especially at the tip where the glass was sealed. And it has a concave meniscus, which indicates some albeit redicilously little contamination...
But yours flows almost like Hg. The inside glass must be VEEEERY clean.
Amazing how just the slightest impurities can mask the true nature of materials.
Our vast semiconductor industry and by extrapolation our digital age would be impossible if we were only able to achieve 99.99% purity...
An operation room is a pig sty in comparison to a semiconductor factory.
Good craftsmanship!!
God tier indeed!
I love everything about this. Thank-you
Holy shit! 👏👏👏👏👏 Dude, this was my first video of yours and it was awesome, I loved it, Fantastic work on the project and the video and how fucking cool is that insane pattern thing it’s doin inside the glass, that’s incredible!! Did You not geek out over that? Now I’m off to binge the rest of your work, I bet it’s all gonna be just as incredible! 🙏🏼 Really appreciate You Man!
Thank you! I definitely geeked about about the patterns in the half molten cesium. I played around with it for quite a while.
That's some of the most epic footage I have ever seen! So beautiful and scary at the same time.
Beautiful video!
What do you recommend for storing a cesium ampule at home?
I was thinking about a steel box with a larger amount of sand surrounding the ampule. Any better or additional ideas for safety?
Thank you! Yes, I think an airtight steel box with some PE foam with a cutout for the vial would be best. So even if the box gets knocked over, the vial will be likely to survive. With sand it would be more likely to break.
Just make sure the foam does not react with the cesium, otherwise pressure could build in the box if the vial breaks and gaseous reaction products are formed.
Thanks for the reply.
Do you have a recommendation of a commercial polymerfoam with these properties (maybe even a supplier)?
My reasoning with sand was that the cesium reacts with sand and gets quenched rather than being oxidized in air and starting a fire.
The cesium would not react with the sand in my experience. Of the steel box is airtight, I don't think it would start a fire, there just not enough oxygen.
There are a lot of suppliers of polyethylene foam on the internet. In my experience PE will not react with cesium.
Beautiful. I will watch it melt and crystalise any time. Thank you. Grateful.
Impressive, well done. Do you worry about any of the cesium making it over and messing up your rotary vane pump and/or oil?
I thought about that. But no. As you can see, the amount of cesium that condensed even at the very beginning of the stainless steel hose is minute. In addition I bent the hose in a circle so cesium atoms making it into the hose would have to hit the walls and condense on their way to the pump.
Is there a specific word for that bespoke distillation glass design you made?
No, not that I know of.
Beautiful chemistry. Such a untamed art with so many probabilities .But when done safely the outcome is like that of a artist
Thanks again for beautiful content !
What a beautiful element! Art imitates life! Thank you for sharing and talking through the process
Is it possible to use an induction coil to hear the ceasium? That would allow potentially fine control over the heating rate, and avoid over heating the glass.
Why not just use your ears?
This process looks dangerous. I imagine seeing this hundreds of years ago would look like magic. The level of skill makes you like a magician. Nice job.
I know very little about the world of chemistry and in particular the metals like this that are most amazing but I can say for certain fear of mercury is nothing after seeing this stuff!
Wow 🤩 this is truly amazing! I clearly have no clue what is going on, but this is one cool project! Science is so fascinating! Love this and glad I have found this channel!!
Forbidden gold
It looks so beautiful.
That's some high level shit. Your channel is underrated. Damn from the technical view this is the same level as chemicalforce. You could improve a little with the video editing but damn this is so impressive from the technical view.
Thank you! Yes, there is a lot of improvement when it comes to editing and filming. But it's always hard to film when you are alone and busy working on something.
You let us see more of the behind the scenes though. I think it’s a great learning opportunity with your explanation along the way
This is an incredible video! never seen something like that!
*This video is a good example of really smart people doing really dumb things. I'm glad I'm not his neighbor*
You sound fun
Absolutely stunning labwork, bravo.....
Thank you!
the b roll of he cesium flowing the the apparatus was really beautiful
Cesium in the ampule looks so beautiful, even more than your glasswork. Great job, man.
This video was a joy to watch.